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G0014 - Technological plasticity studies of the FeAl intermetallic phase-based alloy
Results of hot torsion tests of the Fe-40Al-5Cr-0.2Mo-0.2Zr-0.02B alloy are presented in the paper. The alloy was obtained by melting in an induction furnace. The tests were carried out using a plastometer of the Sataram type in the temperature range of 1123-1273 K and strain rates of 0.06, 0.24, 0.48 and 2.42 s-1 that were close to those used in plastic working processes. In the alloy studied the super-plasticity phenomenon was observed. The shape of the flow curves indicated that dynamic recrystallisation occurred during the super-plastic deformation. This was confirmed by studies of the alloy structure. Also traces of dynamic recovery were observed. The value of the activation energy Q=343 kJ/mol for dynamical recrystallisation is close to the activation energy of aluminium diffusion in the FeAl phase. The results have revealed that cast FeAl-based alloy can be process by superplasic forming in the range 1123-1223 K at strain rates about 1 s-1.
M. Kupka, Intermetallics 12 (2004) 295-302
G0013 - Application des mesures magntiques la mtallurgie
x
E. Alff and Cl. Bronner, Confrence au Cercle d'Etudes des Mtaux (1973) 1-34
G0012 - Recyling cemented carbides without pollution sorting chargeing material for zinc process
x
K. Hirose, I. Aoki, Int. Conf. Process. Mater. Prop., 1st (1993) 845-848
G0011 - High-temperature thermogravimetric analysis. Influence of gas pressure on kinetics of reactions in the solid state
A magnetic balance apparatus has been set up to follow reactions in the solid state under controlled conditions of pressure and temperature (25-1000¡) Magnetic properties are characteristic of solid structures, and thermomagnetic analysis (T. M. A.) can give the variations of the sample susceptibility during the course of a reaction (susceptibilities of the new phases and of initial compounds not yet transformed). By continuous measurement of this susceptibility with the Faraday method, the conversion degree of the synthesis can be obtained. T. M. A. has been used to study the influence of a gas on a solid-solid reaction in which no gas can be evolved or consumed. An example is given for iron tungstate synthesis: Fe203(s) + WO3(s) --> Fe2WO6(s). At 800¡ the reaction kinetics depends on the nature and the pressure of the gas.
G. Thomas and F. Ropital, Journal of Thermal Analysis 30 (1985) 121-128
E0223 - Use of spent pot linings from primary aluminium production as raw materials for the production of opal glasses
The use of the carbonaceous fraction of spent pot linings (SPL) from primary aluminium electrolytic cells as a raw material for the production of opal glasses is evaluated. The SPL was heat treated and mixed with limestone to eliminate carbon and to minimise fluorine volatilisation. This material was then mixed with other glass formers, melted, and quenched to produce a glass. The cyanide which forms part of the SPL was thermally decomposed and some of the fluorine is incorporated into the glass matrix. The final material contains small crystals of fluorspar, which are responsible for light scattering and the opacity of the material, dispersed in an amorphous phase. The crystalline phase was identified by x-ray diffraction and its morphology was observed by scanning electron microscopy
U.S. do Prado, J.R. Martinelli, J.C. Bressiani, Glass Technology - European Journal of Glass Science and Technology Part A, Volume 51, Number 5, October 2010 , pp. 205-208(4)
E0222 - Isomorphism and phase diagram of Pb5(PO4)3FÐPb5(PO4)3Cl system
Compounds of composition Pb5(PO4)3FxCl1?x (0 ² x ² 1), which are synthetic analogues of minerals pyromorphite, flourapatite, and endlichite, were synthesized for the first time by high-temperature solid phase reactions. X-ray diffraction and IR spectroscopy were used to determine the structure of the compounds and revealed complete miscibility in the solid phase of the Pb5(PO4)3FÐPb5(PO4)3Cl binary system. Adiabatic reaction calorimetry was used to measure standard enthalpies of mixing and formation and show that the regular solutions model is applicable to the Pb5(PO4)3FÐPb5(PO4)3Cl system. Differential thermal analysis in tandem with high-temperature X-ray diffraction were used to study the phase diagram and characterize phase transitions.
A.V. Knyazev, N.G. Chernorukov, E.N. Bulanov, Thermochimica Acta 513 (2011) 112Ð118
E0221 - Effect of TiO2 addition on the crystallization and tribological properties of MgOÐCaOÐSiO2ÐP2O5ÐF glasses
The kinetic parameters including the activation energy for crystallization (E), the Avrami parameter (n) and frequency factor (?) of a glass in the MgOÐCaOÐSiO2ÐP2O5ÐF system were studied using non-isothermal differential thermal analysis (DTA) with regard to small amount of TiO2 additions. It has been shown that the role of TiO2 changes from a glass network former to a glass network modifier with increasing TiO2 content in this system. The kinetic parameters of the crystallizing phases, apatite and wollastonite, indicated changes accompanied with TiO2 additions, implying that the TiO2 is an effective nucleating agent for promoting the crystallization of apatite and wollastonite. The most effective addition is of about 4 wt% TiO2 in this system. The wear rate and friction coefficient decreased from 1.8 ± 0.1 to 0.9 ± 0.2 and 0.87 to 0.77, respectively, when 4 wt% TiO2 was incorporated to the base glass
Jongee Park, Abdullah Ozturk, Thermochimica Acta ,470 (2008) 60Ð66
E0220 - Phase diagram of apatite system Ca10(PO4)6Cl2ÐPb10(PO4)6Cl2
Compounds in Ca10(PO4)6Cl2ÐPb10(PO4)6Cl2 system were synthesized by solid state reaction. It was ascertained using DTA and X-ray diffraction methods that in the investigated system there are two fields because of the formation a compound with formula Ca7Pb3(PO4)6Cl2. The first area is the Pb10(PO4)6Cl2ÐCa7Pb3(PO4)6Cl2 which is characterized by unbounded mixing of components. The second Ca7Pb3(PO4)6Cl2ÐCa10(PO4)6Cl2 area has complicated character due to presence of decomposition processes. In spite of the presence of the one nature polymorphic transitions of Ca10(PO4)6Cl2 and Pb10(PO4)6Cl2 the same effects on all solid solutions were not observed
A.V. Knyazev, N.G. Chernorukov, E.N. Bulanov, Thermochimica Acta ,526 (2011) 72Ð77
E0219 - Investigation of Selected Thermo-physical Properties of Ternary Sn-Zn-Al Alloys Using DTA
The paper deals with the investigation of temperatures and latent heats of phase transformations of two binary alloys Sn-Zn and five ternary Sn-Zn-Al alloys using the DTA method. The investigated alloys belong to the area of the so called eutectic ãvalleyÒ of the Sn-Zn-Al system. DTA of investigated samples was performed at the rate of heating/cooling of 4¡C/min. In this way there were obtained temperatures of phase transformations of the ternary system Sn-Zn-Al, temperature of ternary eutectics TE1 197.6¡C, temperature of liquidus, and other transformations. Latent heats of melting and solidification were calculated. Latent heat of melting of alloys varies within the interval 71-91 J?.g-1, solidification within the range 73-99 J?g-1. Theoretical isoplethic phase diagrams were created with use of the software MTData and Pandat. Experimental data were compared with the calculated temperatures. It follows from bibliographic searches that description of behaviour of ternary system Sn-Zn-Al is still not quite known. The Sn-Zn-Al alloys could become a suitable alternative substitute of lead based solders for temperatures up to 350¡C.
Bed?ich Smetana, Simona Zl, Jarom'r Drpala, Ale? Kroupa, Kristina Pe?inov, Rostislav Burkovi?, Ne?elezn kovy a slitiny, Hutnick listy ?.1/2010, ro?. LXIII
E0218 - Phase transformation temperatures of pure iron and low alloyed steels in the low temperature region using DTA
The paper reports a study of temperatures of phase transitions of nine samples of real grades of low-alloyed steels, including one sample of pure iron, using differential thermal analysis. Temperatures of phase transitions were measured in the low-temperature interval (20Ð10008C). Investigated systems were analysed at selected rates of heating/cooling and then temperatures of phase transitions for zero heating/cooling rate were determined. The results obtained are compared with temperatures of the equilibrium metastable diagram FeÐC, with results from the software IDS and with temperatures of phase transitions calculated according to relations published in available literature. It follows from the results that differences, sometimes considerable ones, still exist between experimental and theoretical data, which implies the necessity for further systematic research in this area.
Bedrich Smetana, Simona Zl, Jana Dobrovsk, Petr Kozelsky, Int. J. Mat. Res. (formerly Z. Metallkd.) 101 (2010) 3
E0217 - Contribution lÕtude de la prcipitation des phases intermtalliques dans lÕalliage 718
Many structural alloys are strengthened by the presence of precipitates in the grains or at grain boundaries. Nickel based superalloys often present an austenitic matrix in which ordered intermetallic phases precipitate. In the alloy Inconel 718, one can find ?' L12 cubic ordered precipitates together with the compound Ni3Nb in its metastable form ?" (D022 - tetragonal) or the stable phase ? (D0a - orthorhombic). The incidence of those precipitates on macroscopic properties of the alloy 718 is well known and widely used in industrial applications. However the mechanisms responsible for the precipitation and transformation of these phases are not fully understood, which motivated the present study. The alloy microstructure has been observed by optical microscopy (OM) and electron microscopy (scanning and transmission, SEM and TEM) in the as received state as well as after heat treatment (isothermal and anisothermal). Differential thermal analysis (DTA) was used to determine the precipitation and dissolution temperatures of the phases ?', ?" and ?. Various precipitation microstructures were obtained by heat treatments based on available TTT diagrams. Some of the structural defects present in ?" and ? precipitates have been characterised by lattice imaging TEM observations. It is shown that stacking faults in phase can act as a seed for the germination of ?. The structure of the interface and the orientation defects in lamellae suggest that the growth of phase occurs directly from the matrix (and not by transformation of the ?ÕÕ phase).
Aliou NIANG, Thse Universit de Toulouse, 2010
E0216 - Thermophysical and structural study of IN 792-5A Nickel based superalloy
The presented paper deals with study of phase transformations temperatures of nickel based superalloy IN 792-5A with application of DTA Ð method and use of experimental laboratory system for simultaneous thermal analysis SETARAM Setsys 18TM. Samples taken from as-received state of superalloy were heated with controlled ramp rates (1, 5, 10 and 20 ¡Cámin-1) and immediately after melting they were cooled with the same controlled ramp rate. The samples before and after DTA-analysis were also subjected to the phase analysis with use of scanning electron microscopy on the microprobe (JCXA 733) equipped with energy dispersive analyser EDAX (EDAM 3).
S. Zla, J. Dobrovska, B. Smetana, M. ?aludova, V. Vodarek, K. Konecna, METABK 2010
E0215 - Application of high temperature DTA to micro-alloyed steels
Paper deals with investigation of phase transitions temperatures for selected real grades of micro-alloyed steels. Temperatures of characteristic phase transitions were obtained using Setaram SETSYS 18TM. The DTA technique was selected for the study of micro-alloyed steels. Temperatures of phase transitions (liquidus, solidus etc.) were obtained. Influence of admixed and alloyed elements on shift of temperatures was investigated. Resulting data were compared with temperatures of phase transitions of Fe-C, Fe-Mn systems and with temperatures calculated according to relations published in available literature. Thermodynamic-kinetic solidification model IDS was used to calculate characteristic equilibrium temperatures of investigated systems.
B. Smetana, S. Zla, M. ?aludova, J. Dobrovska, P. Kozelsky, METABK 2010
E0214 - Direct measurements of fusion and phase transition enthalpies in lanthanum oxide
Enthalpies of high-temperature phase transitions and fusion in lanthanum oxide (La2O3) were directly measured for the first time. Three samples were prepared by laser melting, sealed in tungsten crucibles, and heated in a differential thermal analyzer calibrated by melting Al2O3. Transformation enthalpy of La2O3 from A to H phase is 23 ± 5 kJ/mol at 2046 ± 5 ¡C and from H to X phase is 17± 5 kJ/mol at 2114 ± 5 ¡C. Lanthanum oxide melts at 2301 ± 10 ¡C, with enthalpy of fusion of 78 ± 10 kJ/mol.
Sergey V. Ushakova, Alexandra Navrotsky, J. Mater. Res., Vol. 26, No. 7, Apr 14, 2011
E0213 - Crystallization study of NaÐGd phosphate glass using non-isothermal DTA
NaÐGd phosphate glasses doped with Ce3+ are intensively studied due to their high intensity radioluminescence. Crystallization kinetics of glass with nominal composition of NaGd(PO3)4 was investigated using non-isothermal DTA at heating rates between 10 and 115 K minÐ1 and evaluated by the Kissinger and Ozawa peak methods. The activation energy for crystallization was determined for heating rates lower than 72 KminÐ1 as 789.91 and 802.77 kJmolÐ1 by using the Kissinger and Ozawamethods, respectively. Formation of nuclei, their dimensions and movement of the crystallization front were observed using isothermal optical thermomicroscopy
K. Nitsch, M. Rodov, Journal of Thermal Analysis and Calorimetry, Vol. 91 (2008) 1, 137Ð140
E0212 - Effect of Na2O/K2O substitution on thermophysical properties of PbO based phosphate glasses
PbO based phosphate glasses having composition 40P2O5 12Al2O3 6B2O3 9PbO xNa2O (33Ðx)K2O (x=0Ð33) [F=Na/(Na+K)] have been prepared using conventional melt quench technique. Density, morphology, thermal expansion coefficient ( ) and glass transition temperature (Tg) were studied as a function of Na/(Na+K) ratio. Formation of transparent, bubble free and clear glass was observed up to x=18 mol%. Density was found to vary from 2.70 to 3.69 g cmÐ3. The significant changes were noticed in external morphologies at temperatures corresponding to softening, half ball and melting points under high temperature microscope for three compositions (x=0, 10 and 15 mol%). These glasses recorded the softening and half ball temperatures in the range 454Ð470¡C and 523Ð576¡C respectively and melting temperatures agree well with DTA studies within the experimental limits. Glass transition temperature showed a broad maxima while thermal expansion coefficient (TEC) a broad minima around Na/(Na+K)=0.54. This behaviour is explained on the basis of bond formation/phase separation.
K. V. Shah, M. Goswami, D. K. Aswal, V. K. Shrikhande, S. K. Gupta, G. P. Kothiyal, Journal of Thermal Analysis and Calorimetry, Vol. 89 (2007) 1, 153Ð157
E0211 - Phase transition in LAMOX type compounds
La2Mo2O9 (LMO) was synthesized at lower temperature 973 K (LT-phase) by ceramic route. Differential thermal analysis (DTA) scan of LT-phase of LMO showed ??? transition at 843 K during heating and ??? conversion via a metastable g-phase during cooling. This was also confirmed by thermo-dilatometry and impedance spectroscopy. La2Mo1.95V0.05O9Ðd (LMVO), La1.96Sr0.04Mo2O9Ðd (LSMO) and La1.96Sr0.04Mo1.95V0.05O9Ðd (LSMVO) were prepared in a similar way. These compounds exhibited ??? transition on heating with shift in transition temperature, but the existence of ?-phase during cooling disappeared. Substitution increased the ionic conductivity of ?-phase and reduced that of ?-phase.
M. Ali (Basu), B. N. Wani, S. R. Bharadwaj, Journal of Thermal Analysis and Calorimetry, Vol. 96 (2009) 2, 463Ð468
E0210 - Application of high temperature DTA technique to Fe based systems
The paper deals with the study of phase transformation temperatures of Fe (Fe-C) based metallic alloys. Influence of heating/cooling rate and composition on shift of phase transformation temperatures is investigated in this paper. Six samples with graded carbon content were investigated. Plasma and vacuum melting was performed to prepare alloys. Liquidus-solidus and ??? region was studied. Temperatures of phase transformations were obtained using DTA and Setaram Setsys 18TM laboratory system. DTA experiments of prepared alloys were conducted under inert atmosphere (Ar, >6N). Controlled rate of heating/cooling of alloys was conducted: 2, 4, 7, 10, 15, 20 K min-1. Aproximation to the equilibrium conditions was achieved. The extrapolation of obtained phase transformation temperatures to a zero heating/cooling rate was performed. Comparison of obtained experimental data with data presented in the literature and IDS results was carried out. It follows from copmarison of obtained results with accessible data in the literature the lack of these data and differencies between them. The knowledge of simple binary system Fe-C behaviour is important for the description of more complex systems; ternary, quaternary,É and multicomponent (steels) also. This study is the base of wide research activity at our department in the future.
Bed!ich Smetana, Monika ?aludova, Simona Zla, Jana Dobrovska, Michal Cagala, Ivo Szurman, Daniel Petlak, Metal 2010, Roznov pod Radhostem,Czech Republic
E0209 - Investigation of relevant phase diagrams for high temperature solder materials: The binary systems Cu-Sn and Cu-Sb
Although solders in the electronic industry have only a relative small contribution to the worldwide consumption of lead, the recycling of the electronic waste is complicated and thus it pollutes the environment. Therefore the electronic industry has tried to substitute the poisonous lead in the solders for less harmful materials during the last decade. Interested alloys are those ones which could include the components of the lead free solder and the substrate materials. This work concentrates on the experimental research of the binary systems Cu-Sn and Cu-Sb. Experimental techniques are the powder X-ray diffraction at normal and higher temperatures (PXRD / HTPXRD), thermal analysis (DTA) and metallographic methods (EPMA / ESEM).
Siegfried Frtauer, Thesis, University of Vienna, 2010
E0208 - The Structure and Stability of High Temperature Intermetallic Phases for Application within Coating Systems
The reduction of noise and emissions is becoming increasingly important in civil aircraft jet engines as well as requirements for reduced fuel consumption and improved efficiency. This has resulted in the drive towards increasing turbine entry temperatures and the development of thermal barrier coatings (TBCs). Due to the effectiveness of the platinum-modified nickel aluminides currently used as bond coat layers for Ni-based superalloy TBCs, higher temperature ruthenium-containing bond coat layers are being examined as a possible low cost alternative to platinum.The aim of this research was to examine the stability of various phases within platinum and ruthenium-containing multilayer systems formed during the above reaction process and to determine the most stable intermetallics for inclusion in future coating systems. Foil samples were manufactured using multilayer sputter coating methods and the exothermic formation of these phases was examined using differential scanning calorimetry. The identification of the phases formed was carried out using X-ray diffraction.
Tracey Roberts, Thesis, Cranfield University November 2009
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